Amandla ekholomu aqukethe usayizi ongu-1, 3, 6, kanye no-10 ml, njll.
Inqubo yethu yokukhiqiza inciphisa ukuguquguquka futhi ithuthukisa izinqubo zokutakula nokuhlanza
1.C18 I-Octadecyl Endcapped
2.C18 Ukuphela Okungapheli
3.C8 I-Octyl
4.CN I-Cyanopropyl
5. I-Amine ye-PSA Eyinhloko Neyesibili
6.NH2 Aminopropyl
7. I-SAX Strong Anion Exchange
8. I-SCX Strong Cation Exchange
Amakholomu e-Silica base solid-phase extraction (SPE) ayithuluzi elibalulekile emkhakheni we-analytical chemistry, asetshenziselwa ukuhlanza nokukhipha ama-target compounds kusuka kuma-complex sample matrices. Lawa makholomu aklanywe nge-silica-based stationary phase, enikeza ukukhetha okuphezulu kanye nokusebenza kahle enkambisweni yokuhlukanisa.
Amakholomu ethu e-SPE esisekelo se-silica atholakala ngamakholomu ahlukahlukene, kufaka phakathi osayizi abangu-1, 3, 6, kanye no-10 ml, ahlangabezana nezidingo ezahlukene zohlelo lokusebenza. Inqubo yokukhiqiza esetshenziswa kula makholomu iklanywe ngokucophelela ukunciphisa ukuguquguquka nokuthuthukisa izinqubo zokubuyisa nokuhlanza, ukuqinisekisa ukusebenza okulinganayo nokuthembekile.
Isigaba esimile samakholomu ethu e-SPE esisekelo se-silica sitholakala kuhlu lwezinhlobo zamakhemikhali, ngayinye iklanyelwe izidingo ezithile zokuhlukanisa. Lokhu kufaka phakathi i-octadecyl ye-C18 endcapped, i-octadecyl ye-C18 ene-endcapped, i-octyl ye-C8, i-cyanopropyl ye-CN, i-amine ye-primary-secondary ye-PSA, i-aminopropyl ye-NH2, i-SAX strong anion exchange, kanye ne-SCX strong cation exchange. Lolu hlu oluhlukahlukene lwamakhemikhali luvumela ukukhishwa okuphumelelayo nokuhlanzwa kwezinhlobonhlobo zama-analyte, okwenza amakholomu abe nokuguquguquka futhi avumelane nezinselele ezahlukene zokuhlaziya.
Isibonelo, isigaba se-octadecyl esine-C18 endcapped silungele ukugcinwa nokuhlukaniswa kwamakhemikhali angewona ama-polar kanye nama-polar aphakathi nendawo, kuyilapho isigaba se-CN cyanopropyl sinikeza ukukhetha okuthuthukisiwe kwamakhemikhali e-polar. Isigaba se-amine esiyinhloko-sesibili se-PSA sifanelekela ukukhishwa kwamakhemikhali ane-acidic, kanti isigaba se-SAX kanye ne-SCX senzelwe ngqo ukusetshenziswa kokushintshana kwama-ion.
Ngaphezu kokukhetha kwazo okuhlukahlukene, amakholomu ethu e-SPE esisekelo se-silica aziwa ngomthamo wawo ophezulu wokulayisha amasampula, ukuphindaphindeka okuhle kakhulu, kanye namazinga aphansi okubopha okungaqondile, okuqinisekisa imiphumela enembile nethembekile. Kungakhathaliseki ukuthi asetshenziswa ekuhlaziyeni kwemithi, ezemvelo, ukudla, noma kwezomthetho, la makholomu anikeza ukusebenza okuqinile nokuqhubekayo, okuhlangabezana nezidingo zama-laboratory okuhlaziya anamuhla.
Ekuphetheni, amakholomu e-SPE esisekelo se-silica angamathuluzi abalulekile okulungiselela amasampula kumakhemikhali okuhlaziya, futhi uhla lwethu lwamakholomu, anamakhemikhali awo ahlukahlukene kanye nokusebenza okuthembekile, aklanyelwe ukuhlangabezana nezidingo ezahlukahlukene zososayensi bokuhlaziya. Ngokukhetha kwawo okuphezulu, ukusebenza kahle, kanye nomthamo, la makholomu adlala indima ebalulekile ekukhishweni nasekuhlanzweni ngempumelelo kwamakhemikhali aqondiwe kusuka kuma-matrices esampula ayinkimbinkimbi.
**Isihloko: Ukuvula amandla amakholomu e-SPE asekelwe ku-silica ukuze kulungiselelwe isampula ethuthukisiwe**
Emkhakheni we-analytical chemistry, ukubaluleka kokulungiselela amasampula akunakuphikiswa. Elinye lamathuluzi asebenza kahle kakhulu kule njongo yi-silica-based solid phase extraction (SPE) cartridge. Yakhelwe ukwenza lula inqubo yokukhipha, la ma-cartridge atholakala ngamanani ahlukahlukene, kufaka phakathi osayizi abangu-1, 3, 6, kanye no-10 mL, ukuze amukele izinhlobo ezahlukene zamasampula.
Amakholomu ethu e-SPE asekelwe ku-silica aklanywe ngokucophelela ukuqinisekisa ukuguquguquka okuncane ekusebenzeni. Lokhu kubalulekile kubacwaningi nabahlaziyi abathembele emiphumeleni ehambisanayo. Izinqubo zokukhiqiza esizisebenzisayo azigcini nje ngokukhulisa ukubuyiswa kwabahlaziyi abahlosiwe, kodwa futhi zithuthukisa izinqubo zokuhlanza, okwenza kube lula ukuthola amasampula ahlanzekile kakhulu.
Phakathi kwezinketho ezahlukene ezitholakalayo, amakholomu ethu aqukethe izinhlobo ezintathu ezahlukene zezigaba ezimile: i-C18 Endcapped Octadecyl, i-C18 Unendcapped Octadecyl, kanye ne-C8 Octyl. Amakholomu e-C18 Endcapped Octadecyl afaneleka kahle kokubili amakhompawundi e-polar kanye nama-non-polar, anikeza ukugcinwa okuhle kakhulu nokukhetha. Amakholomu e-C18 Unendcapped Octadecyl anikeza izinzuzo ezifanayo kodwa afaneleka ngqo kuma-analyte angewona ama-polar, okuqinisekisa ukusebenza okuhle kakhulu kuzo zonke izinhlelo zokusebenza. Kulabo abasebenza ngamakhompawundi amancane e-polar, amakholomu e-C8 Octyl anikeza indlela elinganiselayo yokufeza ukuhlukaniswa okusebenzayo ngenkathi kugcinwa ukubuyiselwa okuphezulu.
Kungakhathaliseki ukuthi usebenza kwezemithi, ekuhlolweni kwemvelo, noma ekuphepheni kokudla, amakholomu ethu e-SPE asekelwe ku-silica angahlangabezana nezidingo zakho zokuhlaziya. Ngokukhetha ikholomu efanele yesicelo sakho esithile, ungathuthukisa ukusebenza kahle kwenqubo yokulungiselela isampula, okuholela emiphumeleni ethembekile futhi ephindaphindwayo. Zizwe amandla amakholomu e-SPE asekelwe ku-silica namuhla futhi uthuthukise amakhono akho okuhlaziya!